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Description
All samples were serially diluted in assay buffer in duplicate and incubated with cells for 30 min at RT before detection with the cAMP dynamic 2 HTRF assay (Cisbio assays, Bedford, MA) as described previously 51
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How the formulation may be evaluated Laboratory evaluation may focus on the formulation's stability, temperature sensitivity, visual characteristics, delivery-device behaviour and compatibility with analytical testing procedures

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