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Description
The crude peptides were subsequently purified by reverse-phase chromatography on a C18 column with a linear gradient of water and acetonitrile containing 0.1% TFA, and their molecular masses were verified by liquid chromatographymass spectrometry (LC/MS)
This is an important point that often gets lost in the discussionthe trials weren't halted due to catastrophic safety concerns

doi: 10.1007/s10725-005-6324-2 40 LichtenthalerH

Upon receiving the lyophilized peptide, store at 4 C or colder and away from bright light

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