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An Agilent GC 6890 system (Agilent, Waldbronn, Germany) coupled to an FID detector equipped with a capillary HP INNOWAX column (30 m 0.32 mm, 0.5 m coating thickness, Agilent, Waldbronn, Germany) was used, Helium served as carrier gas (30 cm s1), with an injector temperature of 220 C
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