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Helium was used as carrier gas, injection volume was 1 l, injector temperature was 250C, the column temperature was increased from 120 to 240C at a rate of 5C/min, and the GCMS line transfer temperature was 280C

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The conversion of primary BA into their secondary forms involves the transformation of cholate into deoxycholate and the conversion of chenodeoxycholate into lithocholate

In contrast, at low concentration (0.6 M) only with a higher AGC target ( 1 10 6 ) both m/z were detected (Fig

Cell 158 , 8497 (2014)