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There were no clinical signs of toxicity or pathological changes

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The powder may have degraded before reconstitution due to improper storage, high temperature exposure, or moisture infiltration into the sealed vial

Since lyophilization is accomplished by dissolving the substance in a solute to begin with, and Empowerx do not tell what solute they use, (hopefully not benzene) then this obviously accounts for the difference in volume which you have so clearly noted