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Description
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NMR spectral changes

Cracking 100mL of cracking reagent is prepared as TFA EDT TIS H 2 And (3) adding the full protection peptide under the ice-bath condition, returning to the room temperature after 0.5h, continuing to react for 2h, and adding anhydrous ether for precipitation after the reaction is finished

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DOI 10.1016/S0960-9822(00)00336-5
